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Beilstein J. Org. Chem. 2012, 8, 461–471, doi:10.3762/bjoc.8.53
Graphical Abstract
Scheme 1: Preparation of ArSF4Cl 2.
Scheme 2: Preparation of Ar(SF4Cl)n from Ar(SH)n (n = 2, 3).
Scheme 3: Reaction mechanism for the formation of ArSF4Cl.
Scheme 4: Reaction mechanism for the formation of trans and cis-ArSF4Cl.
Scheme 5: Preparation of ArSF5 with ZnF2.
Scheme 6: Preparation of PhSF5 with anhydrous HF.
Scheme 7: Preparation of 3a with HF–pyridine.
Scheme 8: Preparation of polyfluorinated ArSF5.
Scheme 9: Preparation of aryl bis- and tris(sulfur pentafluorides), Ar(SF5)n (n = 2,3).